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Isotope Analysis Service

Infrared Soil Analysis laboratory - Research

About the ISAL | ISAL strengths | Current Research & Applications | In-field Applications | Staff/Contact


History of MIR at CSIRO | What is mid infrared (MIR) spectroscopy? | Predicting soil properties | Statistical Methods & Analysis | Additional Services | Routine Analyses

About the Infrared Soil Analysis Laboratory (ISAL)

CSIRO Land and Water has over 40 years experience in the use of mid infrared (MIR) spectroscopy for research and routine applications.

What we can do

This cost-effective technique can be used to predict a wide range of chemical and physical soil properties quickly and easily, as well as allowing for the examination of soil chemical composition, which is expressed in the infrared spectra.

The MIR method provides a very rapid and useful tool for the investigation of chemical and physical processes important in plant root growth, soil fertility, soil acidity, soil moisture retention, factors determining nutrient and contaminant availability and ecotoxicity. Due to the low cost of the MIR method for soil analysis, it is ideally suited to landscape variability surveys, precision agriculture and contaminated site investigations.

ISAL conducts research and provides fundamental information on soil chemistry, soil organic matter, and soil mineralogy for scientists in Australia and overseas. It assists the development and applications of methods for soil analysis for soil fertility studies, soil physical measurements and contaminants in soils.

The laboratory has access to a broad range of data and computer models for analysing soils, minerals and soil organic matter supporting activities such as soil surveys, environmental monitoring and precision agriculture.

The routine soil analysis capability focuses on rapid and inexpensive turnaround for many soil physical and chemical properties. The ISAL also carries out consulting and project work for commercial clients.

Clients

The ISAL provides research support to groups within and outside CSIRO, and is available to assist and collaborate with industry, government, research institutes and universities.

Equipment

MIR spectrometer

The ISAL is based within the CSIRO Land and Water Analytical Service Unit, Adelaide. It is equipped with a Perkin-Elmer Spectrum One , Fourier-Transform Infrared (FTIR) spectrometer.  Having a spectral range from the NIR 7800cm-1 through to the MIR at 450cm-1. Typically spectra are scanned for one minute at 8cm-1 resolution using a diffuse reflectance (DRIFT) sample accessory. 

The ISAL  also has access to field-portable FTIR spectrometer/s and has alternative sample introduction techniques including Attenuated Total Reflectance (ATR) and Photo-Acoustic Spectroscopy (PAS) for specialised research applications. Samples for DRIFT are usually reduced to a fine powder using a vibrating puck mill for fine grinding, prior to scanning.

The MIR facility also has access to field-portable FTIR spectrometer/s such as A2 Technology's Exoscan and has alternative sample introduction techniques including Attenuated Total Reflectance (ATR) and Photo-Acoustic Spectroscopy (PAS) for specialised research applications. Samples for DRIFT are usually reduced to a fine powder using a vibrating puck mill for fine grinding, prior to scanning.

Analysis

The MIR service has access to a number of software options for spectral processing, multivariate statistical methods such as PLS analysis, and neural networks, including a custom PLS prediction module designed for specific client applications.

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Strengths of the ISAL

The major strengths of the CSIRO ISAL are:

  • Large range of possible analyses
  • Availability of a wide range of infrared accessories and spectrometers, and the expertise to use them
  • MIR expertise developed over 40 years
  • Continuing product development
  • International reputation
  • Extensive collaboration with State and Commonwealth organisations
  • Support from CSIRO researchers and government funding agencies
  • Back-up consulting service available
  • Strong links with industry partners
  • Commercialisation experience

Read more about mid infrared (MIR) spectrometry in relation to soil analysis.

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ISAL current research and applications

Current research and applications at the ISAL include:

  • Soil contamination: Research into contaminants and their interactions with soils, and practical application of rapid infrared techniques for the assessment of contaminated soils.
  • Metal partitioning: The use of ICP-MS and MIR spectrometry to predict metal partition coefficients across Europe.
  • Soil forensics: IR spectroscopy is used in the early stages of soil examination, to either estimate soil chemical and physical characteristics, examination of the spectra to determine similarity of samples prior to further examination via other spectroscopic methods, and to help identify organic components/compounds in unknown samples.
  • Soil composition: The use of infrared techniques to examine soil composition.
  • Soil survey and site assessment: Using rapid infrared techniques, using infrared spectrometry and spectroscopy, to predict soil physicochemical properties, and the investigation of the soils compositional chemistry.
  • Novel method development: The ISAL has recently lodged three provisional patents pertaining to novel ways of detecting contaminants at contaminated sites (Aust prov. patents June 2009 and Feb 2010, US prov. patent Sept 2009) with commercial business partners.

See a list of selected significant publications relevant to MIR.

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ISAL in-field applications

Hand held portable MIR equipment beign used in the fieldsThe ISAL is currently evaluating the robustness and performance of handheld spectrometers for the rapid on-site investigation of soil physical properties, soil nutrients, contaminants in soils and contaminant behaviour. These instruments will allow rapid in-field screening of soils for identification of areas or soils that require more detailed laboratory analysis, and those that do not.

This offers the possibility of rapidly shortening the time for investigations into soil chemical and physical behaviour, and rapid problem identification and management in the field.

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ISAL staff and contact details

  • Sean Forrester, Research Officer, Infrared analyst /spectroscopist, ISAL Manager
  • Les Janik, Principal Scientist, Infrared spectroscopy, soil organic matter, clay mineralogy, consultant
  • Mike McLaughlin, Chief Research Scientist, Applications of IR to soil fertility and soil contamination

For further information contact:
Sean Forrester
CSIRO Land and Water
Private Bag No. 2
Glen Osmond SA 5064
Australia
Tel: +61-8-8303 8527
Fax: +61-8-8303 8565

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